Fe(110) - \(0.05 \; \mathrm{M}\) \(\ce{ Na2SO4 }\)

echemdb identifier: hirai_2000_situ_702_f2_solid
tags: BCV

A cyclic voltammogramm for Fe(110) recorded in \(0.05 \; \mathrm{M}\) \(\ce{ Na2SO4 }\) at a scan rate of \(50 \; \mathrm{mV\,s^{-1}}\) from Figure 2 in N. Hirai et al. In situ electrochemical atomic force microscopy with atomic resolution of Fe\(110\) in sodium sulfate aqueous solution. ISIJ international, 40\(7\):702–705, 2000.

Further information

The figure shows digitized data.

The Fe(110) electrode was prepared by:

• Orientation by Laue backscattering, mechanically polished and etched.
• details see https://doi.org/10.2355/isijinternational.40.702

Metadata

Details on the electrochemical system (yaml)

electrodes:
- function: reference electrode
  material: Hg/Hg2SO4
  name: RE
- crystallographicOrientation: '110'
  function: working electrode
  material: Fe
  name: WE
  preparationProcedure:
    description:
    - Orientation by Laue backscattering, mechanically polished and etched.
    - details see https://doi.org/10.2355/isijinternational.40.702
  purity:
    grade: '99.9'
    unit: pct
  source:
    manufacturer: Monocrystal
  type: Fe single crystal rod
electrolyte:
  components:
  - name: water
    source:
      refinement: Milli-Q
    type: solvent
  - concentration:
      unit: mol / l
      value: 0.05
    name: Na2SO4
    purity:
      grade: Superior
    source:
      supplier: Wako
    type: salt
  ph:
    value: 6.5
  type: aqueous
type: electrochemical

Citation key (bibtex)

@article{hirai_2000_situ_702,
    author = "Hirai, Nobumitsu and Okada, Hiromi and Hara, Shigeta",
    title = "In situ electrochemical atomic force microscopy with atomic resolution of Fe(110) in sodium sulfate aqueous solution",
    journal = "ISIJ international",
    volume = "40",
    number = "7",
    pages = "702--705",
    year = "2000",
    publisher = "The Iron and Steel Institute of Japan"
}

Details about the original figure in the publicaton (yaml).

comment: ''
fields:
- name: E
  orientation: horizontal
  reference: Hg/Hg2SO4
  type: number
  unit: mV
- name: j
  orientation: vertical
  type: number
  unit: mA / cm2
measurementType: CV
scanRate:
  unit: mV / s
  value: 50.0
simultaneousMeasurements: []
type: digitized

Details about the curation process of this entry (yaml).

process:
- date: '2026-01-21'
  name: Valerie Link
  orcid: https://orcid.org/0009-0004-3341-1452
  role: curator

---